LAB TECHNIQUES ORGANIC CHEMISTRY 4E [Paperback]

Laboratory Techniques in Organic Chemistryis the most comprehensive and detailed presentation of the lab techniques organic chemistry students need to know. Compatible with any organic chemistry lab manual or set of experiments, it combines specific instructions for three different kinds of laboratory glassware: miniscale, standard taper microscale, and Williamson microscale. It is written to provide effective support for guided-inquiry and design-based experiments and projects, as well as for traditional lab experiments.PART 1 Introduction to the Organic Laboratory
ESSAY The Role of the Laboratory

1. Safety in the Laboratory
2. Green Chemistry
3. Laboratory Notebooks and Prelaboratory Information

PART 2 Carrying Out Chemical Reactions
ESSAY Learning to Do Organic Chemistry

4. Laboratory Glassware
5. Measurements and Transferring Reagents
6. Heating and Cooling Methods
7. Setting Up Organic Reactions
8. Computational Chemistry

PART 3 Basic Methods for Separation, Purification, and Analysis
ESSAY Intermolecular Forces in Organic Chemistry

9. Filtration
10. Extraction
11. Drying Organic Liquids and Recovering Reaction Products
12. Boiling Points and Distillation
13. Refractometry
14. Melting Points and Melting Ranges
15. Recrystallization
16. Sublimation
17. Optical Activity and Enantiomeric Analysis

PART 4 Chromatography
ESSAY Modern Chromatographic Separations

18. Thin-Layer Chromatography
19. Liquid Chromatography
20. Gas Chromatography

PART 5 Spectrometric Characterization Methods
ESSAY The Spectrometric Revolution

21. Infrared Spectroscopy
22. Nuclear Magnetic Resonance Spectroscopy
23. 13C and Two-Dimensional NMR Spectroscopy
24. Mass Spectrometry
25. Ultraviolet and Visible Spectroscopy
26 . Integrated Spectrometry Problems

PART 6 DlC3