Practical NMR Spectroscopy Laboratory Guide Using Bruker Spectrometers [Paperback]

Practical NMR Spectroscopy Laboratory Guide is designed to provide non-expert NMR users, typically graduate students in chemistry, an introduction to various facets of practical solution-state NMR spectroscopy. Each chapter offers a series of hands-on exercises, introducing various NMR concepts and experiments and guiding the reader in running these experiments using an NMR spectrometer. The book is written for use with a Bruker NMR spectrometer running TopSpin software versions 1 or 2. This practical resource functions both as a text for instructors of a practical NMR course and also as a reference for spectrometer administrators or NMR facility directors when doing user training. This guide serves as serve as excellent, practical resource on its own or as a companion book to Timothy Claridge's? High-Resolution NMR Techniques in Organic Chemistry, 2nd Edition (Elsevier, 2009).

• Written by experts in solution-state NMR spectroscopy
• Provides step-by-step instructions for more than 50 activities using a Bruker NMR spectrometer
• Includes detailed appendices and sample questions for lab reports

Introduction
1. Basics and Spectrometer Performance Checks
2. Multiple Irradiation and Multiple Pulse Experiments
3. Polarization Transfer and Its Applications
4. Homonuclear Correlation Experiments
5. PFG (Pulsed Field Gradient) Experiments
6. Introduction to NMR of Biomolecules in H₂O
7. Selective Experiments Using Shaped Pulses
8. Diffusion Measurements and DOSY (Diffusion Ordered SpectroscopY)Dr. John Simon Harwood has served as Director of the Purdue University Interdepartmental NMR Facility (PINMRF) since 2005, where he has overseen the rationalization and expansion of PINMRF such that the facility now includes two spectrometers with cryoprobes all³*